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Extra info for An Introduction to Spectroscopic Methods for the Identification of Organic Compounds. Nuclear Magnetic Resonance and Infrared Spectroscopy

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ROMEO, Ann. Chim. (Italy), 1960, 50, 1198. 11. J. R. NUNN, / . Chem. , 1952, 313; P. K. FAURE and J. C. SMITH, / . Chem. Soc, 1956, 1818. 12. K. L. RINEHART, W. A. NILSSON, and H. A. WHALEY, / . Amer. Chem. Soc, 1958, 80, 503. 13. S. G. SMITH and S. WINSTEIN, Tetrahedron, 1958, 3, 317. 14. E. W. ABEL, R. P. BUSH, F. J. HOPTON, and C. R. JENKINS, Chem. , 1966, 58. 15. J. M. Cox, J. A. ELVIDGE, and D. E. H. JONES, / . Chem. Soc, 1964, 1423. 16. C. F. CALLIS, J. R. VAN WAZER, J. N. SHOOLERY, and W.

28. The *H resonance spectrum of formamide (a) without spin decoupling, (b) with spin decoupling at the 14 N resonance frequency. , reproduced by permission) the J/δ ratio. (21) Cryogenic magnets are being produced which enable experiments to be performed at 220 MHz for proton studies. 13 13 C H SATELLITES The presence of a C atom in an otherwise symmetrical molecule can sometimes introduce magnetic non-equivalence between nuclei which are equivalent in the 12C containing molecule. The 11 % natural abundance of this spin half isotope allows these satellite bands to be observed in all carbon compounds, and they can often be used as an aid to analysis.

KARPLUS, / . , 1959, 30, 11. 22. J. S. BURTON, J. A. ELVIDGE, and R. STEVENS, J. Chem. Soc, 1964, 3816. 23. 24. 25. 26. F. W. LICHTENTHALER and H. O. L. FISCHER, J. Amer. Chem. Soc, 1961, 83, 2005. S. STERNHELL, Rev. Pure Appl. , 1964, 14, 15. S. FORSÉN and B. ÂKERMARK, Acta Chem. , 1963, 17, 1712. J. A. POPLE, / . Chem. , 1956, 24, 1111; Mol. , 1958,1, 175; R. MCWEENEY, Mol. , 1958,1, 311 ; C. E. JOHNSON and F. A. BOVEY, J. Chem. , 1958, 29, 1012; J. S. WAUGH and R. W. FESSENDEN, /. Amer. Chem.

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